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Beilstein J. Org. Chem. 2017, 13, 1407–1412, doi:10.3762/bjoc.13.137
Graphical Abstract
Figure 1: Main synthetic strategies towards heterocyclic cores of D-series GE2270 and our present one.
Scheme 1: Synthesis of trithiazolylpyridine 9. Reaction conditions: a) Pd(OAc)2 (5 mol %), CyJohnPhos (10 mol...
Scheme 2: Synthesis of chiral thioamide 16. Reaction conditions: a) SnCl2∙2H2O, dioxane/H2O (1:3), 0 °C to rt...
Scheme 3: Synthesis of the heterocyclic core of the D-series GE2270. Reaction conditions: a) TBDMSOTf, NEt3, ...